Measurements of the phosphorus electron Overhauser effect at two magnetic fields are reported for a series of phosphorus chalcogenides in carbon disulphide solutions containing the tri-butylphenoxyl radical. Large positive enhancements were observed for the PIII nuclei. This has enabled the 77Se satellite spectra of P4Se3 to be analysed, and n.m.r. parameters to be obtained for a number of the compounds.
R. A. Dwek, R. E. Richards, D. Taylor, G. J. Penney and G. M. Sheldrick, J. Chem. Soc. A, 1969, 935 DOI: 10.1039/J19690000935
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