Deuteriation of diazoacetone
Abstract
Reaction of CD3·COCl with CH2N2 gives CD3·CO·CHN2; exchange of CH3·CO·CHN2 with D2O in the presence of sodium azide gives CH3·CO·CDN2.
Reaction of CD3·COCl with CH2N2 gives CD3·CO·CHN2; exchange of CH3·CO·CHN2 with D2O in the presence of sodium azide gives CH3·CO·CDN2.
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A. Santucci, A. Foffani and G. Piazza, J. Chem. Soc. D, 1969, 1262b DOI: 10.1039/C2969001262B
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