The signs of 2JPP in cis- and trans-[(OC)4Mo{P(OMe)3}2] were found from double resonance experiments on the 13C satellites in the 1H spectra to be negative and positive, respectively.
R. D. Bertrand, F. Ogilvie and J. G. Verkade, J. Chem. Soc. D, 1969, 756 DOI: 10.1039/C29690000756
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