The determination of nitrite with Cleve's acid has been investigated; the influence of composition of reagents and several experimental conditions have been evaluated. It is shown that provided the standards used to prepare the calibration graph and samples are treated in a similar way, then the choice of conditions may largely be left to the operator. A recommended procedure is given.
N. G. Bunton, N. T. Crosby and S. J. Patterson, Analyst, 1969, 94, 585 DOI: 10.1039/AN9699400585
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