Desulphuration of a number of heterocyclic thiols by treatment with nickel boride in aqueous solution at 200° is reported. Some other were unchanged after similar treatment. Refluxing ethylene glycol provided an alternative reaction medium.
J. Clark, R. K. Grantham and J. Lydiate, J. Chem. Soc. C, 1968, 1122 DOI: 10.1039/J39680001122
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