Species of the type [M(CO)3SR]x(M = Mn, Re) are shown from fundamental and combination infrared spectra to be tetrameric in solution, and to have a regular tetrahedral structure with no metal–metal bonding.
P. S. Braterman, J. Chem. Soc. A, 1968, 2907 DOI: 10.1039/J19680002907
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