Crystallisation of trans-[Rh(4-py·CHO)4Cl2]Cl (py = pyridine) from water has been found to give trans-[Rh(4-py·CH(OH)2)4Cl2]Cl, whereas trans-[Rh(3-py·CHO)4Cl2]Cl·3H2O crystallises from water unchanged.
R. D. Gillard and B. T. Heaton, J. Chem. Soc. A, 1968, 1405 DOI: 10.1039/J19680001405
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