The investigation of the Kolbe and Hofer-Moest reaction by a non-steady state method of applying a sequence of square-wave pulses to the working electrode is discussed. This technique permits the measurement of the formation of all the products of the reaction as a function of time, and allows a more searching evaluation of the reaction mechanisms than steady-state methods alone.
M. Fleischmann and F. Goodridge, Discuss. Faraday Soc., 1968, 45, 254 DOI: 10.1039/DF9684500254
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