A rapid gravimetric method for the determination of uranium dioxide in uranium monophosphide and triuranium tetraphosphide is described. The phosphide compounds are dissolved in an ethyl acetate-hydrochloric acid solution and the remaining uranium dioxide oxidised in air to triuranium octoxide. A precision of ±0·2 per cent. w/v is claimed for each determination.
J. L. Driscoll and P. E. Evans, Analyst, 1968, 93, 403 DOI: 10.1039/AN9689300403
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