The preparation of 3β,16α-dihydroxyandrost-5-ene-11,17-dione (V) and 3β,11β,16α-trihydroxyandrost-5-en-17-one (VI) from 3β-hydroxyandrost-5-ene-11,17-dione (I) is described. A single absorption band of medium intensity in the region 800–820 cm.–1 has been observed in the infrared spectra of four 3β-acetoxy-11-oxo-Δ5-steroids.
R. W. Kelly and P. J. Sykes, J. Chem. Soc. C, 1967, 2082 DOI: 10.1039/J39670002082
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