(±)-7-Hydroxy-6-methoxy-1-(4-methoxybenzyl)-2,8-dimethyl-1,2,3,4-tetrahydroisoquinoline has been synthesised by a conventional route. The i.r., n.m.r., and mass spectra of this material are superposable on those of (–)-hemirepanduline, thus proving the structure of the latter.
K. Aoki and J. Harley-Mason, J. Chem. Soc. C, 1967, 1957 DOI: 10.1039/J39670001957
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