The preparation of 9-phenanthrylamine in high yield, by way of phenanthryne, from 9-bromophenanthrene and sodamide in liquid ammonia is described. The properties of di-9-phenanthrylamine, obtained as a by-product, are compared with those described in conflicting literature reports.
R. H. Altiparmakian and R. S. W. Braithwaite, J. Chem. Soc. C, 1967, 1818 DOI: 10.1039/J39670001818
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