The reaction between tetra-O-acyl-α-(and-β-)D-glucopyranosyl halides and cadmium dialkyls has been used as a basis for the synthesis of the diastereoisomeric 1,2-O-(1-methylpropylidene)-α-D-glucopyranoses. The configurations at the cyclic ketal carbon may be assigned from n.m.r. data.
R. G. Rees, A. R. Tatchell and R. D. Wells, J. Chem. Soc. C, 1967, 1768 DOI: 10.1039/J39670001768
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