The product from the reaction of nitrous acid with NNN′N′-tetramethyl-p-phenylenediamine is N1N1N4-trimethyl-2-nitro-N4-nitroso-p-phenylenediamine, which is also produced by the action of nitrous acid on NNN′-trimethyl-p-phenylenediamine. Unambiguous syntheses of the two isomeric N-trimethyl-nitro-p-phenylenediamines and of NN′-tetramethyl-2-nitro- and NN′-dimethyl-2-nitro-p-phenylenediamine are described.
J. F. Corbett and A. G. Fooks, J. Chem. Soc. C, 1967, 1136 DOI: 10.1039/J39670001136
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