The sulphoxides Ph·[CH2]n·SO·Me (n= 0–4) were compared in pyrolytic and mass spectrometric behaviour. On pyrolysis either β-elimination or rearrangement occurred, but similar effects were not observed in the mass spectra. The attempted preparation of one of the sulphoxides actually yielded the next higher homologue by a complex series of reactions.
I. D. Entwistle, R. A. W. Johnstone and B. J. Millard, J. Chem. Soc. C, 1967, 302 DOI: 10.1039/J39670000302
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