1-O-Methyl-D-mannitol has been prepared by treating 1,2-anhydro-3,4:5,6-di-O-isopropylidene-D-mannitol with sodium methoxide. 2-O-Methyl-D-mannitol has been obtained by stepwise hydrolysis of 1,2,6-tri-O-benzoyl-3,4-O-isopropylidene-D-mannitol, and 3-O-methyl-D-mannitol has been isolated after reduction of 3-O-methyl-D-fructose with Raney nickel.
S. Bayne, J. A. Fewster, A. J. Grieve and M. L. Hawksley, J. Chem. Soc. C, 1967, 114 DOI: 10.1039/J39670000114
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