The absence of detectable coupling between the two kinds of hydrogen atom in dimethyl phosphite necessitates the use of a triple resonance experiment for the determination of the sign of J(31P–1H). J(31C–1H) and J(31P–1H) are found to be of like sign and a technique of “partial decoupling” is described.
W. McFarlane, J. Chem. Soc. A, 1967, 1148 DOI: 10.1039/J19670001148
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