Reaction of tetrafluoroallene with hexafluorobut-2-yne at 80—85° under autogenous pressure in the presence of free-radical scavengers yields, as major product, perfluoro-(1,2-dimethyl-3-methylenecyclobutene), the 19F nuclear magnetic resonance spectrum of which is discussed.
R. E. Banks, W. R. Deem, R. N. Haszeldine and D. R. Taylor, J. Chem. Soc. C, 1966, 2051 DOI: 10.1039/J39660002051
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