The periodate oxidation of some Δ1-pyrroline 1-oxides with two substituents at C-5 but unsubstituted at C-2 leads to a series of 4-nitrosopentanoic acids. Evidence is adduced for the course of the reaction. An N-alkylhydroxyamino-compound is oxidised in chloroform to the nitroso-compound by tetraethylammonium periodate, a potentially useful reagent soluble in various organic solvents.
A. K. Qureshi and B. Sklarz, J. Chem. Soc. C, 1966, 412 DOI: 10.1039/J39660000412
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