Electrolyses of alkoxy(phenyl)acetic acids, in ethanol, give benzaldehyde and benzophenone simple and mixed acetals. The infrared spectra of a number of acetals and ketals are recorded in the 3000 and 1400 cm.–1 regions, and assignments are made for some frequencies. A method for differentiation of dimethyl, diethyl, and ethyl methyl acetals, as well as between benzaldehyde acetals and benzophenone ketals, is suggested.
B. Wladislaw, A. Giora and G. Vicentini, J. Chem. Soc. B, 1966, 586 DOI: 10.1039/J29660000586
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