We demonstrate how different modes of guest binding with a Co8L12 cubic cage can be determined using ESI-MS. High stoichiometry guest binding was observed, with the guests preferentially binding externally, but internal guest inclusion was also seen at higher guest loading.
D. L. Stares, C. Mozaceanu, M. D. Ward and C. A. Schalley, Chem. Commun., 2023, 59, 11811 DOI: 10.1039/D3CC04291J
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