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General and versatile electrochemical α-C(sp3)–H amidation for N-Mannich base synthesis

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A regioselective synthesis of β-difluoromethoxy vinyl sulfonesvia O-difluoromethylation of β-ketosulfones using sodium chlorodifluoroacetate

Km Ishu, Neha Sharma Prabhakar and Krishna Nand Singh

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Recent advances and applications of electrochemical mass spectrometry for real-time monitoring of electrochemical reactions

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Microdroplet Accelerating C(sp2)–H Halogenation in Organic, Pharmaceutical, Analytical, and Environmental Use

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Electrochemical α‐Functionalization of N‐Aryl‐Activated Tertiary Amines

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Fluorescence spectroelectrochemistry for the study of electrochemiluminescence of the CdTe quantum dots/tripropylamine coreactant system

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Mild Diarylmethylation of Indoles through Regioselective 1,6-Hydroarylation of para-Quinone Methides in Microdroplets/Thin Film

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Radical dehydroxylative C-glycosylation of 1-hydroxycarbohydrates enabled by photoredox catalysis

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Dual C2 Synthon Strategy for the Synthesis of Pyrimidines: Copper‐Catalyzed Aerobic α,β‐C(sp3)−H Bond Difunctionalization of Tertiary Alkylamines

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Adv Synth Catal, 2025, 367
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Electrochemically Driven Ugi-Azide Reaction via C(sp3)–H Bond Activation of Tertiary Amines

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Direct Synthesis of β-Amino Boronates via Amide α-C–H Bond Activation and C(sp3)–C(sp3) Coupling under Dual Ni/Photoredox Catalysis

Zihao Hu, Dong Wang and Tao XU

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Photocatalytic and electrocatalytic α-C–H functionalization of tertiary amines

Yumeng Liu, Xiaojian Li and Jiahong Li

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Rapid Mass Spectrometric Identification of the Radical Intermediates in Nanozyme-Catalyzed Reactions Using a Tip-Based Microreactor

Liu Qu, Hong-Yuan Chen, Jun Hu and Jing-Juan Xu

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Electrochemical Desaturation and β-Thiocyanation of Cyclic Amides

Kaili Miao, Jin Zhang, Jiaxin Chen, Lin-Bao Zhang, Ming Li, Lirong Wen and Weisi Guo

Org. Lett., 2025, 27, 186
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Insights into electrogenerated intermediates and rapid screening of electrochemical reactions by surface-modified carbon fiber paper redox spray ionization mass spectrometry

Jiahui Bai, Mingmai Bao, Shanshan Wang, Tianlun Wen, Yuling Li, Jing Zhang, Tiansheng Mei and Yinlong Guo

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Paired electrolysis enables para-C–H amination of phenols with nitroarenes and mechanistic visualization via multifunctional electrochemical mass spectrometry

Tianjiao Peng, Ziyue Chen, Xi Cui, Hanning Jiang, Yongyi Li, Zhenwei Wei, Aiwen Lei and Hong Yi

Nat Commun, 2026
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