Issue 51, 2024

Elimination of homogeneous broadening in 1H solid-state NMR

Abstract

1H solid-state NMR spectra are plagued by low resolution, necessitating the use of complex pulse sequences or specialized equipment. We introduce a new resolution enhancement method, inspired by super-resolution microscopy, that uses a 2D Hahn-echo experiment to constrain deconvolution. The result is an effective doubling of the MAS frequency.

Graphical abstract: Elimination of homogeneous broadening in 1H solid-state NMR

Article information

Article type
Communication
Submitted
06 may 2024
Accepted
31 may 2024
First published
03 iyn 2024

Chem. Commun., 2024,60, 6552-6555

Elimination of homogeneous broadening in 1H solid-state NMR

F. A. Perras, Chem. Commun., 2024, 60, 6552 DOI: 10.1039/D4CC02191F

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