A green method for regioselective hydrophosphinylation of α,β-unsaturated ketones using alkylaluminium compounds has been developed. It proceeds without acids, bases, or additives, yielding γ-ketophosphine oxides efficiently. This process offers excellent atom economy, functional group tolerance, and high yields in a short time.
Y. Chen, Z. Pang, G. Li, X. Yang, W. Yan, Q. Li, X. Dong, X. Ma and Z. Yang, Chem. Commun., 2025, 61, 9666 DOI: 10.1039/D5CC01440A
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