Issue 82, 2013
From the journal:

Chemical Communications

A facile synthesis of UiO-66, UiO-67 and their derivatives†

Michael J. Katz,‡a   Zachary J. Brown,‡a   Yamil J. Colón,b   Paul W. Siu,a   Karl A. Scheidt,a   Randall Q. Snurr,b   Joseph T. Hupp*a  and  Omar K. Farha*a  

* Corresponding authors

a Department of Chemistry, Northwestern University, 2145 Sheridan Road, Evanston, Illinois 60208, USA
E-mail: o-farha@northwestern.edu, j-hupp@northwestern.edu
Tel: +1-847-491-3504

b Department of Chemical & Biological Engineering, Northwestern University, 2145 Sheridan Road, Evanston, Illinois 60208, USA

Abstract

A scalable, reproducible method of synthesizing UiO-66- and UiO-67-type MOFs, entailing the addition of HCl to the reaction mixture, has been investigated. The new protocol requires a fraction of the time of previously reported procedures, yields exceptional porosities, and works with a range of linkers.

Graphical abstract: A facile synthesis of UiO-66, UiO-67 and their derivatives

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Article information

DOI
https://doi.org/10.1039/C3CC46105J
Article type
Communication
Submitted
09 Leq 2013
Accepted
28 Leq 2013
First published
06 Way 2013

Chem. Commun., 2013,49, 9449-9451

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A facile synthesis of UiO-66, UiO-67 and their derivatives

M. J. Katz, Z. J. Brown, Y. J. Colón, P. W. Siu, K. A. Scheidt, R. Q. Snurr, J. T. Hupp and O. K. Farha, Chem. Commun., 2013, 49, 9449 DOI: 10.1039/C3CC46105J

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