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Issue 37, 2020
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Low-power STMAS – breaking through the limit of large quadrupolar interactions in high-resolution solid-state NMR spectroscopy

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Abstract

An STMAS NMR experiment requiring significantly lower rf fields is presented, allowing acquisition of high-resolution spectra for half-integer spins regardless of the magnitude of their quadrupolar interaction. The experiment relies on frequency crossings induced by sample spinning during ‘long’ rf pulses to coherently cover the satellite-transitions efficiently.

Graphical abstract: Low-power STMAS – breaking through the limit of large quadrupolar interactions in high-resolution solid-state NMR spectroscopy

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Article information


Submitted
12 Aug 2020
Accepted
15 Sep 2020
First published
21 Sep 2020

Phys. Chem. Chem. Phys., 2020,22, 21119-21123
Article type
Paper

Low-power STMAS – breaking through the limit of large quadrupolar interactions in high-resolution solid-state NMR spectroscopy

I. Hung and Z. Gan, Phys. Chem. Chem. Phys., 2020, 22, 21119
DOI: 10.1039/D0CP04274A

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