Treatment of cyanoethylated tetrathiafulvalene-thiolates or cyanoethylated 1,3-dithiole-2-thione-4,5-dithiolate with one equiv. of caesium hydroxide hydrate selectively and in high yield produces the corresponding monocaesium salts, which can subsequently be alkylated.
J. Becher, J. Lau, P. Leriche, P. Mørk and N. Svenstrup, J. Chem. Soc., Chem. Commun., 1994, 2715 DOI: 10.1039/C39940002715
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