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Journal cover: Organic & Biomolecular Chemistry

Organic & Biomolecular Chemistry

Rapid publication of high quality organic chemistry research
Impact Factor 3.562 48 Issues per Year Indexed in Medline
 
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Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00283H, Paper
One of the shortest synthetic routes to L-iduronic acid derivatives is via free radical reduction of the C-5 bromide of the corresponding protected D-glucuronic acid derivative. The epimerization of such...
 
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C5OB02659H, Paper
An efficient chemoselective domino oxidative homocoupling of 2-aminoaryl ketone in presence of 2-iodoxybenzoic acid (IBX) for the synthesis of iminoquinone has been developed. The domino reaction proceeds via three consecutive...
 
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00058D, Perspective
Glycosyltransferase-catalyzed enzymatic and chemoenzymatic syntheses are powerful approaches for the production of oligosaccharides, polysaccharides, glycoconjugates, and their derivatives. Enzymes involved in the biosynthesis of sugar nucleotide donors can be combined...
 
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00170J, Paper
The rhodium catalyzed annulation of anilines with alkynic esters providing for the high yield synthesis of quinoline carboxylates with excellent regioselectivity is described. This unprecedented reaction employs either formic acid...
 
Anne-Sophie Marques, Maxime Giardinetti, Jérôme Marrot, Vincent Coeffard, Xavier Moreau and Christine Greck
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C5OB02437D, Communication
An efficient multicatalytic strategy for the construction of nitrogen-containing heterocycles has been reported. The powerful combination of organic and metal catalysis in a single vessel allowed the formation of enantioenriched...
 
Tamara Beisel, Johannes Kirchner, Tanja Kaehler, Julia Knauer, Yashar Soltani and Georg Manolikakes
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00108D, Communication
From themed collection New Talent
A Brønsted acid-catalyzed addition of 2-alkylazaarenes to in situ generated N-sulfonylimines through selective C(sp3)–H bond functionalization has been developed. This protocol provides an atom- and step-economic approach to α-substituted sulfonamides.
 
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00179C, Paper
Herein we reported a novel iridium(III)-catalyzed ortho-mono-alkynylation of 7-azaindoles under mid conditions. This approach provides a general and straight forward access to form novel 7-azaindole derivatives with ample substrate scope...
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02394G, Paper
Neocuproine based PNAzymes with further conjugated entities as well as constructs clamping the target RNA to form a triplex are reported. This extends the arsenal of PNAzymes as efficient artificial RNA restriction nucleases.
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02620B, Paper
The 6-oxo-5,6-dihydrodibenzo[b,h][1,6]naphthyridine-11-carboxamides were synthesized via a domino reaction as the two bromine atoms in mucobromic acid were found missing.
 
Máté Kicsák, Miklós Bege, Ilona Bereczki, Magdolna Csávás, Mihály Herczeg, Zoltán Kupihár, Lajos Kovács, Anikó Borbás and Pál Herczegh
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C6OB00067C, Communication
A synergistic effect of BF3·Et2O, hexafluoroisopropanol and triethylsilane led to efficient detritylation of nucleoside, monosaccharide and amino acid derivatives.
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C6OB00131A, Paper
Intending to synthesize ω,ω-difluoroalkyl amino acid derivatives by oxidative desulfurization–fluorination reactions of suitable arylthio-2-phthalimido butanoates and pentanoates, in addition to small amounts of the target products, mainly α,ω-polyfluorinated amino acid derivatives were formed by additional sulfur-assisted α-fluorination.
 
Mark Anthony Olson, Marco S Messina, Jonathan R Thompson, Trenton J Dawson, Amanda N Goldner, Daryl K Gaspar, Mariela Vazquez, Jessica A Lehrman and Andrew C.-H. Sue
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00109B, Paper
From themed collection New Talent
Reversible template-directed micellar-size and shape modulation by virtue of host-guest reversible docking of molecular templates at the micellar-solvent interface was achieved in water. By combining a π-electron deficient bipyridinium-based gemini...
 
Benyi Shi, Zhouhe Zhu, Yi-Shuo Zhu, Dagang Zhou, jinyuan wang, Panpan Zhou and huanwang jing
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00102E, Paper
Highly efficient one-pot synthesis of imidazo[2,1-b]thiazole derivatives has been developed by a ring-opening and ring-closing reconstruction of imidazo[2,1-b][1,3,4]thiadiazoles with phenylacetylene in the presence of potassium tert-butoxide (t-BuOK) under very mild...
 
Errika Voutyritsa, Alexis Theodorou and Christoforos G Kokotos
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00036C, Paper
From themed collection New Talent
An efficient and green method for the α-hydroxylation of ketones has been developed. This method includes the in situ conversion of variοus ketones into the corresponding silyl enol ethers and...
 
Goreti Ribeiro Morais, Bradley R. Springett, Martin Pauze, Lisa Schröder, Matthew Northrop and Robert A. Falconer
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C6OB00230G, Paper
Novel strategies for the synthesis of sialosyl and glycosyl disulfides are reported.
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02667A, Paper
From themed collection New Talent
A simple and efficient iodine-assisted protocol for synthesis of 5-substituted-3-methyl/benzyl-1,3,4-oxadiazol-2(3H)-ones has been developed.
 
Jeff Van Raden, Evan Rashied Darzi, Lev Zakharov and Ramesh Jasti
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00133E, Paper
From themed collection New Talent
A highly-strained, nitrogen-doped cycloparaphenylene (CPP), aza[6]CPP, was synthesized and then converted to a donor-acceptor nanohoop, N-methylaza[6]CPP, via alkylation of the nitrogen center. The energy levels of the lowest unoccupied molecular...
 
Jian Lei, Jinbo Huang and Qiang Zhu
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00087H, Review Article
Much attention has been paid in imidoyl radical-involved reactions in recent years. As a divergent reactive intermediate, imidoyl radicals are used for the synthesis of functionalized heterocycles, nitriles, amides, or...
 
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C6OB00156D, Paper
An expeditious and cost-efficient method for synthesis of 1-aryl-cycloprop-2-ene-1-carboxamides was developed. This one-pot protocol involving coupling of amines with acyl chlorides, generated upon treatment of cyclopenylcarboxylic acids with oxalyl chloride,...
 
Aldo Galeone, Veronica Esposito, Antonietta Pepe, Rosanna Filosa, Luciano Mayol and Antonella Virgilio
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C5OB02358K, Paper
G-quadruplex structures formed by oligodeoxyribonucleotides TGGUNH2GGT (AM, UNH2 = 5-amino-2'-deoxyuridine), TGGUBrGGT (BR, UBr = 5-bromo-2'-deoxyuridine) and TGGTGGT (TH) have been investigated through circular dichroism, nuclear magnetic resonance, gel electrophoresis and...
 
Congrong Liu, Lianghui Ding, Guang Guo, Weiwei Liu and Fu-Lai Yang
Org. Biomol. Chem., 2016, Accepted Manuscript
DOI: 10.1039/C5OB02569A, Communication
A novel method to synthesis 2-arylindoles is demonstrated via direct arylation of indoles with arylsulfonyl hydrazides. Under the optimized reaction conditions, the reaction well tolerates a wide variety of functional...
 
A. H. St. Amant, C. P. Frazier, B. Newmeyer, K. R. Fruehauf and J. Read de Alaniz
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C6OB00073H, Communication
From themed collection New Talent
A one-pot synthesis of anilines and nitrosobenzenes from phenols has been developed using an ipso-oxidative aromatic substitution (iSOAr) process.
 
M. J. Durán-Peña, M. E. Flores-Giubi, J. M. Botubol-Ares, L. M. Harwood, I. G. Collado, A. J. Macías-Sánchez and R. Hernández-Galán
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02617B, Paper
A new method for the chemo- and stereoselective conversion of acyclic allylic alcohols into the corresponding substituted cyclopropane derivatives has been developed using lithium carbenoids.
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02616D, Paper
Two diastereomers of optically active N,O-containing new macrocycles with dual chirality were synthesized and evaluated for chiral discrimination of organo phosphoric and phosphonic acids by 31P NMR and fluorescence spectroscopy.
 
Org. Biomol. Chem., 2016, Advance Article
DOI: 10.1039/C5OB02600H, Communication
A catalyst/solvent-free, one-pot and operationally simple method for the synthesis of quinoline-substituted α-hydroxy carboxylic derivatives by the hydroxyheteroarylation of olefins with quinoline N-oxides is reported.
 
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