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CrystEngComm

Design and understanding of solid-state and crystalline materials
Impact Factor 4.034 48 Issues per Year
 
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CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01422K, Paper
A comprehensive solid-state screening experiment was performed for Icariin (ICA), an active substance in Chinese Traditional Medicine (TCM) that has long been used to treat osteroporosis. Two new polymorphs in...
 
Alexander S. Romanov, Gary F. Angles, Alexey V. Shapovalov, Tatiana Timofeeva, Maddalena Corsini, Stefania Fusi and Fabrizia Fabrizi de Biani
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01111F, Paper
Four N-substituted 2,6-(E,E)-bis(ferrocenylidene)piperid-4-ones (NH 1, NMe 2, NEt 3, NCH2Ph 4) were prepared by aldol condensation between ferrocenecarbaldehyde and two equivalents of N-substituted piperid-4-ones with high yields. The N-protonated compounds...
 
Umesh D Pete, Amol G. Dikundwar, vaishali M Sharma, Shridhar P. Gejji, Ratnamala S. Bendre and Tayur N Guru Row
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01156F, Communication
A hitherto unseen rotation of isopropyl group in the solid state, predicted to be forbidden based on theoretical investigations, is reported. This C-C rotation observed during temperature dependant single-crystal-to-single-crystal transformation...
 
Tao Peng, Tieliang Zhao, Qing Zhou, Hongyan Zhou, Jun Wang, Jinyuan Liu and qi liu
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01324K, Paper
NiCo2S4/Ketjen Black nanocomposites have been successfully fabricated on nikcel foam by a facile two-step solution-based method. Compared with the pure NiCo2S4 electrode (Ni1K0), the NiCo2S4/KB nanocomposite electrodes (Ni1K0.5, Ni1K0.25, Ni1K0.125)...
 
Yoshitaka Nakagawa, Hiroyuki Kageyama, Riho Matsumoto, Yuya Oaki and Hiroaki Imai
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01257K, Communication
Uniformly sized Mn3O4 nanocuboids were produced in the presence of tiny round grains ~3 nm in diameter covered with oleic acid in toluene. The formation of the rectangular nanocrystals surrounded...
 
Yong Wang, Hanglong Wu, Hengbo Li, Jun Li, Bin Lu, Yueke Yang, Wentao Yuan and Ze Zhang
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01283J, Communication
We report a facile organic-free hydrothermal strategy to fabricate rutile TiO2 single crystals with a new type of curved surfaces, which consist of high-energy-facet-bound nano-hills rather than quasi-continuous miller-index microfacets....
 
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01088H, Paper
The crystal structures of di-O-Propoxy-mono-Formyl-thiacalix[4]arene∙chloroform (7∙CHCl3), di-O-Propoxy-di-Formyl-thiacalix[4]arene (8), di-O-Propoxy-tri-Formyl-thiacalix[4]arene (9), di-O-Benzyol-di-Formyl-thiacalix[4]arene∙water (10∙H2O), mono-O-Propoxy-tri-Formyl-thiacalix[4]arene (11), di-O-Propoxy-di-Cyano-thiacalix[4]arene•chloroform (12∙CHCl3) in the same crystallisation medium have been investigated. These crystals form similar ‘honeycomb’ nanotubes...
 
Lee Martin, Songjie Yang, Andrew C. Brooks, Peter N. Horton, Louise Male, Ourida Moulfi, Lydie Harmand, Peter Day, William Clegg, Ross W. Harrington and John D. Wallis
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01430A, Paper
Triiodides are arranged in head to tail pairs, infinite lines or a castellated arrangement in the radical cation salts of chiral bis(N(1-arylethyl))pyrrolo-tetrathiafulvalene salts.
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01069A, Highlight
The application of weaker intermolecular attractions to the formation of crystals with desired physical and chemical properties is described. Representative structural examples are analysed critically and approaches are outlined for the future development of this important area.
 
Ik Jae Park, Dong Hoe Kim, Won Mo Seong, Byung Suh Han, Gill Sang Han, Hyun Suk Jung, Mengjin Yang, Wen Fan, Sangwook Lee, Jung-Kun Lee and Kug Sun Hong
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01165E, Paper
Water content in an anodic electrolyte affects the crystallization route of anodic TiO2 nanotube arrays during annealing, which determines the crystallographic orientation of the nanotubes.
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01452B, Paper
Cu(I)/Ag(I) sulfonate CPs have been synthesized and characterized. One of the CPs exhibits a reversible anion exchange for perchlorate and permanganate.
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01220A, Paper
Grid-type hydrogen bonding networks of organic cations are used to capture pseudo-spherical Keggin-type anionic clusters.
 
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01013F, Paper
The molecular-scale understanding of the mechanism through which solvent interacts with the crystal surface during crystal growth process is still a formidable challenge. The quantitative understanding at this venture has...
 
Hong-Chen Yu, Hui-Yuan Wang, Lei Chen, Feng Liu, Cheng Wang and Qi-Chuan Jiang
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01271F, Paper
Primary Mg2Si with a truncated octahedral morphology and size over a range of 8–15 μm were prepared by simultaneously adding Ca and Sb into the Al–Mg–Si melt.
 
Xinyuan Zhang, Xingxing Jiang, Yin Li, Zheshuai Lin, Guochun Zhang and Yicheng Wu
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01006C, Paper
Two isoxazolone-based nonlinear crystals exhibit large SHG responses about 2.8 and 1.5 times that of OH1.
 
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01213A, Paper
Multi-component crystals – salts, co-crystals, or solvates - are usually designed based on the analysis of complementarity of functional groups and intermolecular interactions of the components. However, no crystal design...
 
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01596K, Communication
Boron hydrides typically contain both bridging B-H-B and terminal B-H bonds, which behave respectively as local Lewis acidic and basic sites. Their condensed phases are then stabilised through dihydrogen bonds...
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01379H, Paper
In situ powder XRD investigation of the mechanisms of Ca(OH)2 dehydration and high temperature carbonation, focusing especially on the “superheating” phenomenon.
 
Wenjuan Bian, Ting Wang, Yanmei Guo, Xue Yu, Xuhui Xu and Jianbei Qiu
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01040C, Paper
Upconversion (UC) photoluminescent nanocrystals of Ln3+-doped KLu3F10 have been synthesized via a facile and environmentally-friendly hydrothermal route.
 
Y. N. Palyanov, I. N. Kupriyanov, Y. M. Borzdov and Y. V. Bataleva
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01265A, Paper
High-pressure synthesis of silicon-doped diamond from the Mg–Si–C system is demonstrated. The effects of Si on the crystallization and spectroscopic characteristics of diamond are established.
 
Mei-Feng Wu, Ting-Ting Shen, Shuai He, Ke-Qin Wu, Shuai-Hua Wang, Zhi-Fa Liu, Fakun Zheng and Guo-Cong Guo
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01347J, Communication
Herein, we report a novel high-dimensional I3O3 organic-inorganic hybrid framework, namely [Cd3(OH)2(tza)2]n (1) (H2tza = 1H-tetrazolate-5-acetic acid), where a rare pure ths inorganic connectivity of Cd–Ohydroxyl is observed. Meanwhile, 1...
 
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01350J, Communication
Tailoring the morphologies of metal nanoparticles especially that with concave profiles is still a big challenge for the current syntheses. Here, we report a facile and robust approach for the...
 
Belén Fernández, José M Seco, Javier Cepeda, Antonio Jesús Calahorro and Antonio Rodriguez-Dieguez
CrystEngComm, 2015, Accepted Manuscript
DOI: 10.1039/C5CE01521A, Paper
A series of zinc(II) or cadmium(II) based compounds with elongated dicarboxylate and bipyridine ligands, namely, {dma[Cd(µ-azdc)(µ-ac)]•xDMF}n (1), {[Cd2(µ4-azdc)(µ-azdc)(DMSO)4]•DMSO}n (2), [Cd3(µ4-azdc)3(DMF)2]n (3), {[Zn2(µ3-azdc)2(µ-pbptz)]•xDMF}n (4), and {[Zn3(µ4-azdc)3(µ-pbptz)2]•xDMF•yH2O}n (5) (where dma = dimethylammonium,...
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01205H, Communication
The ternary phase diagram for the direct assembly of a 2 : 1 co-crystal of benzoic acid–sodium benzoate was illustrated. Benzoic acid acted as a reactant and underwent neutralization to produce sodium benzoate. The excessive amount of benzoic acid as an API can interact with the product, sodium benzoate as another API, to undertake API–API co-crystallization by cooling.
 
CrystEngComm, 2015, Advance Article
DOI: 10.1039/C5CE01239B, Paper
Six Co(II) complexes have been hydrothermally synthesized with mixed ligands. The effects of the polycarboxylates on the structures of the title complexes have been discussed.
 

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