The first total synthesis and absolute configuration assignment of asperilactone B (I) have been accomplished. Additionally, a revision of the absolute stereochemistry of asperilactone C has been done. The first total synthesis of the opposite enantiomer of asperilactone B (ent-I) has also been achieved, as well as that of C-7 epimers of both asperilactones B (8) and C (9).
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S. Djokić, G. Benedeković, J. Kesić, M. V. Rodić, M. Popsavin, V. Popsavin and J. Francuz, Org. Biomol. Chem., 2024, 22, 4864 DOI: 10.1039/D4OB00583J
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