A high yielding and operationally simple protocol affords multi-decagram quantities of the synthetically useful methyl but-2-ynoate from commercially available starting materials and reagents.
B. Darses, I. N. Michaelides and D. J. Dixon, Org. Chem. Front., 2014, 1, 117 DOI: 10.1039/C3QO00072A
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