Step-by-step synthesis of one Fe6 wheel and two Fe10 clusters derived from a multidentate triethanolamine ligand

Sui-Jun Liu; Song-De Han; Ji-Min Jia; Li Xue; Yu Cui; Shu-Ming Zhang; Ze Chang

doi:10.1039/C3CE42381F

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Step-by-step synthesis of one Fe₆ wheel and two Fe₁₀ clusters derived from a multidentate triethanolamine ligand†

Sui-Jun Liu,^a Song-De Han,^a Ji-Min Jia,^a Li Xue,^a Yu Cui,^a Shu-Ming Zhang^b and Ze Chang*^a

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* Corresponding authors

^a Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), Department of Chemistry, TKL of Metal- and Molecule-Based Material Chemistry and Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Nankai University, Tianjin 300071, PR China
E-mail: changze@nankai.edu.cn
Fax: +86 22 23502458

^b School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin 300130, PR China

Abstract

One Fe₆ wheel and two Fe₁₀ clusters were obtained with a step-by-step strategy. The wheel and cluster complexes were synthesized by reacting Fe₃O precursors with triethanolamine. A magnetic investigation indicates that the Fe₆ wheel shows strong antiferromagnetic behavior.

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Article information

DOI: https://doi.org/10.1039/C3CE42381F
Article type: Communication
Submitted: 21 Nov 2013
Accepted: 28 Mar 2014
First published: 28 Mar 2014

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CrystEngComm, 2014,16, 5212-5215

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Step-by-step synthesis of one Fe₆ wheel and two Fe₁₀ clusters derived from a multidentate triethanolamine ligand

S. Liu, S. Han, J. Jia, L. Xue, Y. Cui, S. Zhang and Z. Chang, CrystEngComm, 2014, 16, 5212 DOI: 10.1039/C3CE42381F

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