An efficient method for the synthesis of phosphoric fluoride via oxidative coupling between hydrophosphine oxide and NaF is reported. DDQ serves as the oxidizing reagent as well as the hydrogen acceptor. The process involves a Cu(II) catalysis and exhibits great functional group tolerance under mild reaction conditions.
N. Liu, L. Mao, B. Yang and S. Yang, Chem. Commun., 2014, 50, 10879 DOI: 10.1039/C4CC04830J
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