Dichlorination of olefins with NCS/Ph3P

Yasumasa Kamada; Yuta Kitamura; Tetsuaki Tanaka; Takehiko Yoshimitsu

doi:10.1039/C3OB27345H

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Dichlorination of olefins with NCS/Ph₃P†

Yasumasa Kamada,^a Yuta Kitamura,^a Tetsuaki Tanaka^a and Takehiko Yoshimitsu*^a

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* Corresponding authors

^a Graduate School of Pharmaceutical Sciences, Osaka University, 1-6 Yamadaoka, Suita, Osaka 565-0871, Japan
E-mail: yoshimit@phs.osaka-u.ac.jp
Fax: +81-6-6879-8214
Tel: +81-6-6879-8213

Abstract

A 2 : 1 mixture of NCS and Ph₃P successfully promoted the anti-dichlorination of olefins to provide corresponding dichlorides, serving as a molecular chlorine surrogate generated in situ.

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Article information

DOI: https://doi.org/10.1039/C3OB27345H
Article type: Communication
Submitted: 03 Dec 2012
Accepted: 14 Jan 2013
First published: 30 Jan 2013

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Org. Biomol. Chem., 2013,11, 1598-1601

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Dichlorination of olefins with NCS/Ph₃P

Y. Kamada, Y. Kitamura, T. Tanaka and T. Yoshimitsu, Org. Biomol. Chem., 2013, 11, 1598 DOI: 10.1039/C3OB27345H

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Organic & Biomolecular Chemistry