Issue 7, 2003

Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

Abstract

The solvothermal reaction of elemental zinc with sulfur in ethylenediamine (en) as solvent yields [ZnSĀ·0.5(NH2CH2CH2NH2)], 1, an unprecedented ethylenediamine pillared ZnS layered compound, containing two dimensional (2-D) boat-type 6-membered rings, which was characterized by ab initio structure solution from powder diffraction data (SDPD).

Graphical abstract: Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

Supplementary files

Article information

Article type
Communication
Submitted
26 Nov 2002
Accepted
17 Jan 2003
First published
10 Mar 2003

Chem. Commun., 2003, 886-887

Ab initio structure study from in-house powder diffraction of a novel ZnS(EN)0.5 structure with layered wurtzite ZnS fragment

X. Ouyang, T. Tsai, D. Chen, Q. Huang, W. Cheng and A. Clearfield, Chem. Commun., 2003, 886 DOI: 10.1039/B212335P

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