Issue 5, 2002
From the journal:

Green Chemistry

Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

Yong Zhi Jin,a   Noriyuki Yasudaa  and  Junji Inanaga*a  

* Corresponding authors

a Institute for Fundamental Research of Organic Chemistry (IFOC), Kyushu University, Hakozaki, Higashi-ku, Fukuoka, Japan
E-mail: inanaga@ms.ifoc.kyushu-u.ac.jp

Abstract

Silica gel was found to be an excellent medium for the aldehyde-selective Horner-Wadsworth-Emmons reaction, which proceeds at room temperature in a short period of time under solvent-free conditions. The silica gel used for the reaction can be recovered and reused many times without losing its activity.

Graphical abstract: Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

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Article information

DOI
https://doi.org/10.1039/B205239C
Article type
Paper
Submitted
29 May 2002
First published
24 Sep 2002

Green Chem., 2002,4, 498-500

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Organic synthesis in solid media. Solvent-free Horner–Wadsworth–Emmons reaction in silica gel

Y. Z. Jin, N. Yasuda and J. Inanaga, Green Chem., 2002, 4, 498 DOI: 10.1039/B205239C

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