Issue 11, 1999
From the journal:

Chemical Communications

Synthesis and reactivity of the osmium methylidene complex [(C5Me5)Os([double bond, length half m-dash]CH2)(dppm)][OTf]

Julia L. Brumaghim  and  Gregory S. Girolami  

Abstract

Treatment of the hydride complex (C5Me5)Os(dppm)H, [dppm = bis(diphenylphosphino)methane] with 2 equivalents of methyl trifluoromethanesulfonate (MeOTf) affords the methylidene complex [(C5Me5)Os([double bond, length half m-dash]CH2)(dppm)][OTf]; the molecular structure and dynamic NMR behavior of this methylidene complex are described.

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Article information

DOI
https://doi.org/10.1039/A901644I
Article type
Paper

Chem. Commun., 1999, 953-954

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Synthesis and reactivity of the osmium methylidene complex [(C5Me5)Os([double bond, length half m-dash]CH2)(dppm)][OTf]

J. L. Brumaghim and G. S. Girolami, Chem. Commun., 1999, 953 DOI: 10.1039/A901644I

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