The reaction of iron(III) perchlorate with 4-pyridinecarbaldehyde under hydro(solvo)thermal conditions affords bis(isonicotinato)iron(II) 1, in which both pyridine and carboxylate groups coordinate to iron centers resulting in an unprecedented neutral, three-dimensional polymeric network with a carboxylate-bridged Fe–Fe infinite chain.
R. Xiong, S. R. Wilson and W. Lin, J. Chem. Soc., Dalton Trans., 1998, 4089 DOI: 10.1039/A806499G
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