A niobium K edge EXAFS study on the green solutions obtained following hydrolysis of NbCl3(dme) in aqueous non-oxidising strong acids has shown that the major species resulting in these solutions is the incomplete cuboidal chloride-capped triangular niobium cation, [Nb3(µ3-Cl)(µ-O)3(OH2)9]4+.
D. T. Richens and I. J. Shannon, J. Chem. Soc., Dalton Trans., 1998, 2611 DOI: 10.1039/A804247K
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