V-loaded β zeolites can be prepared by a two-step post-synthesis method which consists of first creating vacant T-sites by dealumination of the β zeolite with nitric acid, then contacting them with an ammonium metavanadate solution; the SiOH consumption and the nature of the incorporated V species are characterized by IR, UV–VIS and 29Si MAS NMR spectroscopies.
S. Dzwigaj, M. J. Peltre, P. Massiani, A. Davidson, M. Che, S. Dzwigaj, P. Massiani, T. Sen and S. Sivasanker, Chem. Commun., 1998, 87 DOI: 10.1039/A704556E
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