A convenient synthesis of the (5R)-diastereomer of (+)-goniofufurone 5 from D-mannose has been completed. A key step is the intramolecular PdCl2-catalysed oxidative cyclisation of hydroxy(vinyl)furan 6 to lactol 16.
H. Babu Mereyala, R. Reddy Gadikota and R. Krishnan, J. Chem. Soc., Perkin Trans. 1, 1997, 3567 DOI: 10.1039/A703905K
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