The reaction of [Yb(η-C5Me5)2(OEt2)] with 1 equiv. of [Li{Si(SiMe3)3}(thf)3] in toluene affords [Yb(η-C5Me5){Si(SiMe3)3}(thf)2]1 in high yield; a single-crystal X-ray analysis and multinuclear 171Yb and 29Si NMR spectroscopic data for 1 are reported.
M. M. Corradi, A. D. Frankland, P. B. Hitchcock, M. F. Lappert and G. A. Lawless, Chem. Commun., 1996, 2323 DOI: 10.1039/CC9960002323
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