Trioxabicyclononadienes 2 and 4, easily obtained by addition of nucleophiles to the stable α-oxoketene 1, are transformed into the corresponding 2,4,6,8-tetraoxaadamantanes 3 and 5 in high yields by acid-catalysed hydrolysis.
W. Heilmayer, T. S. Dalvi, C. O. Kappe, C. Wentrup, K. Gruber, H. Sterk and G. Kollenz, J. Chem. Soc., Chem. Commun., 1995, 797 DOI: 10.1039/C39950000797
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