The reduction of dimesitylphenylborane and its substituted analogues with Na–K alloy or K-mirror in THF produces their dianions, the spectral data of which suggest novel structures possessing boron–carbon double bonds with negative charges on the boron and carbon at the para-position in the phenyl ring.
K. Okada, T. Kawata and M. Oda, J. Chem. Soc., Chem. Commun., 1995, 233 DOI: 10.1039/C39950000233
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