Issue 7, 1994

Real-time in situ X-ray diffraction of intercalation reactions

Abstract

Real-time in situ energy dispersive X-ray powder diffraction techniques have been developed to monitor the intercalation of a guest species into a solid host; the time dependence of the extent of reaction (α) for the intercalation of cobaltocene CoCp2(Cp =η5-C5H5) by SnS2 has been experimentally determined and is consistent with a model involving nucleation followed by two-dimensional diffusion of the metallocene molecules into the host lattice.

Article information

Article type
Paper

J. Chem. Soc., Chem. Commun., 1994, 809-810

Real-time in situ X-ray diffraction of intercalation reactions

S. M. Clark, J. S. O. Evans, D. O'Hare, C. J. Nuttall and H. Wong, J. Chem. Soc., Chem. Commun., 1994, 809 DOI: 10.1039/C39940000809

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