Electrospray mass spectrometry gives direct insight into the metal complexes present in solutions of ligands L1, L2and Cul ions and into the self-assembly of the capped complex1; the results agree with UV–VIS spectrophotometric titration data.
E. Leize, A. Van Dorsselaer, R. Krämer and J. Lehn, J. Chem. Soc., Chem. Commun., 1993, 990 DOI: 10.1039/C39930000990
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