Issue 6, 1993
From the journal:

Journal of the Chemical Society, Chemical Communications

Preparation and structure of a disilarhodacycle, fac-[Rh(SiMe2CH2CH2SiMe2)H(PMe3)3]

Kohtaro Osakada,   Kouji Hataya,   Yoshiyuki Nakamura,   Masako Tanaka  and  Takakazu Yamamoto  

Abstract

Treatment of [Rh(SPh)(PMe3)3], prepared in situ from [RhCl(PMe3)n(n= 3, 4) and NaSPh, with 1,2-bis(dimethylsilyl)ethane gave a mixture of cis,mer-[RhH2(SPh)(PMe3)3]1 and fac-[R[graphic omitted]Me2)H(PMe3)3]2; the structure of 2 has been determined by X-ray crystallography.

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Article information

DOI
https://doi.org/10.1039/C39930000576
Article type
Paper

J. Chem. Soc., Chem. Commun., 1993, 576-577

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Preparation and structure of a disilarhodacycle, fac-[Rh(SiMe2CH2CH2SiMe2)H(PMe3)3]

K. Osakada, K. Hataya, Y. Nakamura, M. Tanaka and T. Yamamoto, J. Chem. Soc., Chem. Commun., 1993, 576 DOI: 10.1039/C39930000576

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