cis-Cyclophane-like tetrathiafulvalenes (TTF)7 or 8 with two sulphur atoms linked at the 4 and 4′ positions of the two dithiole moities of the TTF are efficiently obtained from 4-thioxo-mesoionic dithioles; if the linking bridge is too small (less than 8 atoms) a cage-like bis-TTF 9 is obtained.
F. Bertho-Thoraval, A. Robert, A. Souizi, K. Boubekeur and P. Batail, J. Chem. Soc., Chem. Commun., 1991, 843 DOI: 10.1039/C39910000843
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