A rapid high yielding synthesis of N-t-butoxycarbonyl-1-amino-2-oxo-3-oxabicyclo[3.1.0]hexane is described; the synthesis relies on an intramolecular carbenoid reaction of an appropriate malonate derivative followed by Curtius degradation to give the unprotected amino group.
A. M. P. Koskinen and L. Muñoz, J. Chem. Soc., Chem. Commun., 1990, 1373 DOI: 10.1039/C39900001373
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