SCHEDULED MAINTENANCE
[Os3(CO)12] is converted on the surface of partially dehydroxylated MgO under 1 bar of flowing CO at 550 K into [Os5C(CO)14]2–; this one-step synthesis is far simpler and gives much higher yields (65%) than the conventional synthesis.
A. S. Fung, P. A. Tooley, M. J. Kelley and B. C. Gates, J. Chem. Soc., Chem. Commun., 1988, 371 DOI: 10.1039/C39880000371
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